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However, this should not be confused with the melting point of a crystalline substance or the extreme softening of a thermoplastic polymer In a thermoset material at Tg, the relative mobility of the cross-linked polymer molecules changes Below Tg, they are immobile and the material is rigid; above Tg, the relative mobility of the molecules increases and slight movements are possible, which leads to a loss of mechanical strength in the material Although all of the methods described in this section enable us to determine a specific glass transition temperature for laminate materials, it also needs to be emphasized that the glass transition in thermoset resins is not a single defined temperature It usually occurs within a temperature range (for some resin systems, the range can span as much as 100 C), and the Tg is determined within this range.

In addition, the difference between Tg and Td must be pointed out here Tg is the temperature at which mechanical properties of the material change, whereas Td is the temperature where the material starts to irreversibly degrade If one wants to assess a laminate s capability to withstand high-temperature lead-free processing temperatures, Td is the more relevant measure Tg is relevant when assessing loss of mechanical strength which can lead to PCB warpage, bowing, and increased z-axis expansion, which in turn can have a significant impact on PCB reliability..

(5.26)

There are a number of different measurement techniques to determine the Tg. The most commonly used methodologies are thermal analysis techniques. Other techniques are available (such as spectral analysis and electrical characterization), but their use is limited and therefore they will not be discussed here. The three thermal analysis methods that will be discussed in this section are as follows:

Differential scanning calorimetry (DSC) Thermomechanical analysis (TMA) Dynamic mechanical analysis (DMA)

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All of these techniques measure slightly different property changes in the laminate material and therefore the values that are obtained will be different They usually will follow this simple rule of thumb: Tg (DMA) > Tg (DSC) > Tg (TMA) 125211 Tg by Thermomechanical Analysis (TMA) Thermomechanical analysis measures dimensional changes in a material as it is heated from room temperature to a preset final temperature The change in length (width or height) of the specimen with the change in temperature determines the CTE of the materialAt Tg, the expansion coefficient of the material changes and it is this property change that is used to determine the Tg by TMA The test procedure is specified in IPC-TM-650, method 2424C The specimen should have a minimum thickness of 0.

51 mm and at least two samples taken from random locations in the material need to be tested Any copper cladding needs to be removed by etching The treatment of the copper foil leaves a negative imprint on the laminate surface, which can lead to problems during the measurement right below the actual glass transition temperature Therefore, the surface of the specimen should be sanded lightly prior to testingThe edges of the sample should also be smooth and burr-free Use care to minimize stress or heat on the specimen The samples need to be preconditioned for 2 hours at 105 C (221 F), then cooled to room temperature in a desiccator The actual measurement should be started at a temperature no higher than 35 C (95 F); an initial temperature of 23 C is recommended Unless otherwise specified, a scan rate of 10 C (18 F) per min.

is commonly used The temperature ramp needs to be continued at least 30 C (54 F) above the anticipated transition region The Tg is defined as the temperature at which the two tangent lines for the thermal expansion coefficient intersect Figure 125 shows an example of a typical TMA scan The material has a Tg of 1367 C It is recommended to retest the same sample after allowing it to cool down to room temperature to determine whether the measured value for Tg2 is comparable to the measured value of Tg1 If Tg1 is significantly lower than Tg2, then this could be an indication that the sample material was not fully cured when it was tested the first time If Tg1 is significantly higher than Tg2, that could indicate that the sample material has already started to decompose and was approaching Td.